Agrégation chimie Montrouge

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Détail d'une référence bibliographique pour les travaux pratiques et montages

D.W. Mayo, R.M. Pike, D.C. Forbes - Microscale Organic Laboratory With Multistep and Multiscale Syntheses (2015)

Titre  Page   Fichier   Note 
 Reduction of ketones using a metal hydride reagent: 4-t-butyl-cyclohexanol   158     - 
 Photochemical isomerization of an alkene: trans-1,2-dibenzoylethylene   163     - 
 The Cannizzaro reaction with 4-chlorobenzaldehyde   174     - 
 The Cannizzaro reaction with 4-chlorobenzaldehyde (Microwaves)   184     - 
 Isolation and characterization of an optically active natural product: usnic acid   224     - 
 Isolation and characterization of a natural product: caffeine and caffeine 5-nitrosalicylate   232     - 
 Isolation of a natural product by steam distillation: cinnamaldehyde from cinnamon   242     - 
 Hydroboration-oxidation of an alkene: octanol   250     - 
 Diels-Alder reaction: 4-cyclohexene-cis-1,2-dicarboxylic acid anhydride   257     - 
 Diels-Alder reaction: 9,10-dihydroanthracene-9,10-α,β-succinic acid anhydride   269     - 
 Grignard reaction with a ketone: triphenylmethanol   275     - 
 Grignard reaction with an aldehyde: 4-methyl-3-heptanol   284     - 
 The Perkin reaction: condensation of rhodamine with an aromatic aldehyde   289     - 
 Wittig reaction: (E)-stilbene by the instant ylide method   302     - 
 Wittig reaction: methylene-4-tert-butylcyclohexane   307     - 
 Wittig reaction: (E)-stilbene by the Horner-Wadsworth-Emmons reaction   309     - 
 Wittig reaction: trans-9-(2-phenylethenyl)anthracene   309     - 
 Aldol reaction: dibenzalacetone   309     - 
 Quantitative analysis of Grignard reagents: 1-methylbutylmagnesium bromide and phenylmagnesium bromide   317     - 
 Williamson synthesis of ethers: propyl p-tolyl ether and propyl p-tolyl ether   321     - 
 Quantitative analysis of Grignard reagents: phenylmagnesium bromide   324     - 
 Williamson synthesis of ethers: methyl p-ethylphenyl ether   331     - 
 Amide synthesis: acetanilide   342     - 
 Amide synthesis: N,N'-diacetyl-1,4-phenylenediamine   344     - 
 Imide synthesis: maleanilic Acid   349     - 
 Imide synthesis: N-phenylmaleimide   351     - 
 Diazonium coupling reaction: methyl red   358     - 
 Friedel-Craft acylation: acetylferrocene and diacetylferrocene   361     - 
 Aromatic nitration: 5-nitrosalicylic acid   382     - 
 Aromatic nitration: 2- and 4-nitrophenol   384     - 
 Nucleophilic aromatic substitution: 2,4-dinitrophenylthiocyanate   388     - 
 Halogenation using N-bromosuccinimide: 9-bromoanthracene   390     - 
 Hypochlorite oxidation of an alcohol: cyclohexanone   394     - 
 9-fluorenone-2,4-dinitrophenylhydrazone   403     - 
 Hypochlorite oxidation of methyl ketones: benzoic acid   403     - 
 Hypochlorite oxidation of methyl ketones: p-methoxybenzoic Acid   408     - 
 Photochemical isomerization: azobenzene   411     - 
 Diborane reductions: thioxanthene   419     - 
 Diborane reductions: xanthene   420     - 
 Heterocyclic ring synthesis: benzimidazole   425     Aniline : à éviter 
 Heterocyclic ring synthesis: 4-hydroxycoumarin   431     - 
 Heterocyclic ring synthesis: dicoumarol   433     - 
 Grignard and aryl cross-coupling: 1-Methyl-2-(methyl-d3)-benzene   435     - 
 Oxidative coupling of 2-naphthol   442     - 
 Tetraphenylcyclopentadienone   445     - 
 Beckmann rearrangement: benzanilide   446     - 
 (E)-Stilbene (Wittig)   449     - 
 Bromination of (E)-stilbene: meso-stilbene dibromide   452     Brome ? 
 Preparation of an enol acetate: cholesta-3,5-dien-3-ol acetate   453     - 
 Dehydrohalogenation of meso-stilbene dibromide: diphenylacetylene   457     - 
 The benzoin condensation of benzaldehyde: benzoin   468     - 
 Preparation of a polyamide: nylon-6,6   471     - 
 Copper(II) ion oxidation of benzoin: benzil   473     - 
 The Verley-Doebner Modification of the Knoevenagel reaction: trans-cinnamic acid   521     - 
 Bromination of trans-cinnamic acid: erythro-2,3-dibromo-3-phenylpropanoic acid   525     - 
Dernière mise à jour : le 5 juin 2025     home